The resin for VOCs treatment is a styrene-divinylbenzene-based macroporous adsorption resin with a good mesh structure and high specific surface area. It selectively adsorbs organic molecules through the sieving effect of pore size, intermolecular force or hydrogen bonding. It can be applied to the adsorption and recovery of volatile organic compounds (VOCs) at high, medium and low concentrations to achieve the standard emission.